Next-generation disulfide stapling: reduction and functional re-bridging all in one

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Next-generation disulfide stapling: reduction and functional re-bridging all in one.

Herein we present a significant step towards next-generation disulfide stapling reagents. A novel class of reagent has been designed to effect both disulfide reduction and functional re-bridging. The strategy has been applied to great success across various peptides and proteins. Moreover, application to a multi-disulfide system resulted in functional re-bridging without disulfide scrambling.

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Next-generation disulfide stapling: reduction and functional re-bridging all in one† †Electronic supplementary information (ESI) available: 1H and 13C NMR spectra for all small molecules, LC-MS, SDS-PAGE gels and UV-Vis analysis (where applicable) for all bioconjugates. See DOI: 10.1039/c5sc02666k Click here for additional data file.

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ژورنال

عنوان ژورنال: Chemical Science

سال: 2016

ISSN: 2041-6520,2041-6539

DOI: 10.1039/c5sc02666k